The construction and performance characteristics of carbon paste electrodes for Oxomemazine Hydrochloride (OXCl) are described. Different methods for electrode fabrication (modified with the ion-pair, ion pairing agent or soaking the plain electrode in the ion-pair suspension) have been used. Matrix compositions were optimized on the basis of effects of type and content of the modifier as well as influence of the plasticizers. The fabricated electrodes worked satisfactorily in the concentration range from 1×10-6 to 0.001 M with Nernestian cationic slopes, depending on the method of electrode fabrication. The ion-pair modified electrode showed the best performance (slope 57.7 ± 2.1 mV decade-1) compared with the plain electrodes or modified with sodium tetraphenylborate (NaTPB) and fast response time of about 15 s and adequate lifetime (6 weeks). The developed electrodes have been successfully applied as well as end point indicator electrode for the potentiometric titration of OXCl with high accuracy and precision.
| Published in | American Journal of Applied and Industrial Chemistry (Volume 1, Issue 1) |
| DOI | 10.11648/j.ajaic.20170101.14 |
| Page(s) | 14-21 |
| Creative Commons |
This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited. |
| Copyright |
Copyright © The Author(s), 2017. Published by Science Publishing Group |
Oxomemazine HCl, Pharmaceutical Analysis, Ion-Selective Electrodes, Carbon Paste Electrodes, Potentiometry Titration
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APA Style
Yousry M. Issa, Sayed A. Ahmed, Nabila S. Mohamed, Naglaa M. Mohamed. (2017). The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride. American Journal of Applied and Industrial Chemistry, 1(1), 14-21. https://doi.org/10.11648/j.ajaic.20170101.14
ACS Style
Yousry M. Issa; Sayed A. Ahmed; Nabila S. Mohamed; Naglaa M. Mohamed. The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride. Am. J. Appl. Ind. Chem. 2017, 1(1), 14-21. doi: 10.11648/j.ajaic.20170101.14
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Download@article{10.11648/j.ajaic.20170101.14,
author = {Yousry M. Issa and Sayed A. Ahmed and Nabila S. Mohamed and Naglaa M. Mohamed},
title = {The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride},
journal = {American Journal of Applied and Industrial Chemistry},
volume = {1},
number = {1},
pages = {14-21},
doi = {10.11648/j.ajaic.20170101.14},
url = {https://doi.org/10.11648/j.ajaic.20170101.14},
eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajaic.20170101.14},
abstract = {The construction and performance characteristics of carbon paste electrodes for Oxomemazine Hydrochloride (OXCl) are described. Different methods for electrode fabrication (modified with the ion-pair, ion pairing agent or soaking the plain electrode in the ion-pair suspension) have been used. Matrix compositions were optimized on the basis of effects of type and content of the modifier as well as influence of the plasticizers. The fabricated electrodes worked satisfactorily in the concentration range from 1×10-6 to 0.001 M with Nernestian cationic slopes, depending on the method of electrode fabrication. The ion-pair modified electrode showed the best performance (slope 57.7 ± 2.1 mV decade-1) compared with the plain electrodes or modified with sodium tetraphenylborate (NaTPB) and fast response time of about 15 s and adequate lifetime (6 weeks). The developed electrodes have been successfully applied as well as end point indicator electrode for the potentiometric titration of OXCl with high accuracy and precision.},
year = {2017}
}
TY - JOUR T1 - The Construction and Performance Characteristics of Carbon Paste Electrodes for Oxomemazine Hydrochloride AU - Yousry M. Issa AU - Sayed A. Ahmed AU - Nabila S. Mohamed AU - Naglaa M. Mohamed Y1 - 2017/04/01 PY - 2017 N1 - https://doi.org/10.11648/j.ajaic.20170101.14 DO - 10.11648/j.ajaic.20170101.14 T2 - American Journal of Applied and Industrial Chemistry JF - American Journal of Applied and Industrial Chemistry JO - American Journal of Applied and Industrial Chemistry SP - 14 EP - 21 PB - Science Publishing Group SN - 2994-7294 UR - https://doi.org/10.11648/j.ajaic.20170101.14 AB - The construction and performance characteristics of carbon paste electrodes for Oxomemazine Hydrochloride (OXCl) are described. Different methods for electrode fabrication (modified with the ion-pair, ion pairing agent or soaking the plain electrode in the ion-pair suspension) have been used. Matrix compositions were optimized on the basis of effects of type and content of the modifier as well as influence of the plasticizers. The fabricated electrodes worked satisfactorily in the concentration range from 1×10-6 to 0.001 M with Nernestian cationic slopes, depending on the method of electrode fabrication. The ion-pair modified electrode showed the best performance (slope 57.7 ± 2.1 mV decade-1) compared with the plain electrodes or modified with sodium tetraphenylborate (NaTPB) and fast response time of about 15 s and adequate lifetime (6 weeks). The developed electrodes have been successfully applied as well as end point indicator electrode for the potentiometric titration of OXCl with high accuracy and precision. VL - 1 IS - 1 ER -
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