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Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin

Received: 2 April 2016     Accepted: 12 April 2016     Published: 11 May 2016
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Abstract

Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.

Published in American Journal of Applied Chemistry (Volume 4, Issue 3)
DOI 10.11648/j.ajac.20160403.13
Page(s) 84-90
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2016. Published by Science Publishing Group

Keywords

Novolac, Resol, Phenolic Oligomer, Mechanical Properties, SEM

References
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  • APA Style

    Mahendrasinh Raj, Lata Raj. (2016). Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. American Journal of Applied Chemistry, 4(3), 84-90. https://doi.org/10.11648/j.ajac.20160403.13

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    ACS Style

    Mahendrasinh Raj; Lata Raj. Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. Am. J. Appl. Chem. 2016, 4(3), 84-90. doi: 10.11648/j.ajac.20160403.13

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    AMA Style

    Mahendrasinh Raj, Lata Raj. Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin. Am J Appl Chem. 2016;4(3):84-90. doi: 10.11648/j.ajac.20160403.13

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  • @article{10.11648/j.ajac.20160403.13,
      author = {Mahendrasinh Raj and Lata Raj},
      title = {Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin},
      journal = {American Journal of Applied Chemistry},
      volume = {4},
      number = {3},
      pages = {84-90},
      doi = {10.11648/j.ajac.20160403.13},
      url = {https://doi.org/10.11648/j.ajac.20160403.13},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.20160403.13},
      abstract = {Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.},
     year = {2016}
    }
    

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  • TY  - JOUR
    T1  - Synthesis and Characterization of Composite Material Based on Modified Phenolic Resin
    AU  - Mahendrasinh Raj
    AU  - Lata Raj
    Y1  - 2016/05/11
    PY  - 2016
    N1  - https://doi.org/10.11648/j.ajac.20160403.13
    DO  - 10.11648/j.ajac.20160403.13
    T2  - American Journal of Applied Chemistry
    JF  - American Journal of Applied Chemistry
    JO  - American Journal of Applied Chemistry
    SP  - 84
    EP  - 90
    PB  - Science Publishing Group
    SN  - 2330-8745
    UR  - https://doi.org/10.11648/j.ajac.20160403.13
    AB  - Acid and base catalyzed polycondensationreaction of phenol and bisphenol A with crotonaldehyde and cardanol results in novolac and resol type phenolic resins. Phenolic oligomers are characterized by their viscosity, average molecular weight and FT-IR spectral studies. Glass reinforced composites of all phenolic oligomers were prepared. Composites are characterized by their synergetic thermal stability by Thermo gravimetric analysis (TGA), Differential scanning calorimery (DSC), Scanning electron microscopy (SEM), and mechanical properties such as flexural strength, impact strength and hardness, chemical resistance, fibre content over a broad range of compositions. The thermal and curing behavior of the resins are found to vary markedly with the mole ratio and the purity of crotonaldehyde or cardanol. Composites prepared from these resin having very good mechanical properties.
    VL  - 4
    IS  - 3
    ER  - 

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Author Information
  • Polymer Science & Technology Department, Institute of Science &Technology for Advanced Studies& Research (ISTAR), VallabhVidyanagar, Anand, Gujarat, India

  • Chemistry Department, C.N.P.F Arts and D.N Science College, Dabhoi, Vadodara, Gujarat, India

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