Area Function for Nanoindentation at High Temperatures

Toshiro Okawa; Ian Thomas Clark; Katsuhiko Tashiro; Hideo Honma; Kazuhiro Yoshihara; Osamu Takai

doi:doi:10.11648/j.ijmsa.20190806.11

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Area Function for Nanoindentation at High Temperatures

Toshiro Okawa, Ian Thomas Clark, Katsuhiko Tashiro, Hideo Honma, Kazuhiro Yoshihara, Osamu Takai

Published in International Journal of Materials Science and Applications (Volume 8, Issue 6)

Received: 7 October 2019 Accepted: 24 October 2019 Published: 31 October 2019

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Abstract

It becomes important to measure mechanical properties of local area of materials because of downsizing of industrial materials, and the fracture of materials often starts at the nanoscale defects. Therefore, the measurement of hardness of the local area of materials is one of key technologies to develop new materials. Nanoindentation is the depth sensing indentation method and can measure the mechanical properties of nanoscale area of materials. The hardness of materials under the controlled environment like high temperature is a big issue in energy or environment industries. Therefore, it becomes important to measure high temperature mechanical properties of nanoscale area of materials by nanoindentation. However, the shape of indenter may change when an indenter contacts to the material surface at high temperatures, and the nanoindentation at high temperatures may lead to inaccuracy of measurements. Nanoindentation does not measure indented are directly but converts the indentation depth to the indented area by area function. In order to correctly convert the indentation depth to the indented area, it is necessary to derive the area function of indented area at high temperatures. In this report, the area function is proposed that considers the change of indenter shape during repeating contact at heated materials. By using this proposed area function, nanoindentation hardness and the reduced modulus of sapphire were obtained at 303K, 473K, 673K, 873K and 1073K successfully. The nanoindentation can be used at high temperatures, if this proposed area function is used.

Published in	International Journal of Materials Science and Applications (Volume 8, Issue 6)
DOI	10.11648/j.ijmsa.20190806.11
Page(s)	98-102
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2019. Published by Science Publishing Group

Keywords

Nanoindentation, Area Function, Hardness, Elastic Modulus, Sapphire, High Temperature

References

[1]	W. C. Oliver and G. M. Pharr, J. Mater. Res., 7, 1564 (1992).
[2]	Ehab Z. Alsayed, Ilnaz Hariri, Syozi Nakashima, Yasushi Shimada, Turki A. Bakhsh, Junji Tagami, Alireza Sadr, Dental materials, 32 (6), 807 (2016).
[3]	J. J. Roa, G. Fargas, A. Mateo and E. Jiménez-Piqué, Mater. Sci. Eng., 645, 188 (2015).
[4]	A. leitner, V. Maier-Kiener and D. Kiener, Mater. Res. Lett., 5 (7), 486 (2017).
[5]	K. Kesea, P. A. T. Olsson, A.-M. Alvarez Holston and E. Broitman, J. Nucl. Mater., 487, 113 (2017).
[6]	J. M. Wheelerand J. Michler, Rev. Sci. Instrum., 84 101301 (2013).
[7]	J. M. Wheeler, D. E. J. Armstrong, W. Heinz and R. Schwaiger, Curr. Opin. Solid State Mater. Sci., 19 (6), 354 (2015).
[8]	M. Peters, C. Leyens, U. Schulz and W. A. Kaysser, Adv. Eng. Mater., 3, 193 (2001).
[9]	D. R. Clarke and C. G. Levi, Annu. Rev. Mater. Res., 33, pp. 383 (2003).
[10]	Gianni Campatelli and Antonio Scippa, Procedia CIRP, 55, 200 (2016).
[11]	Jonathan C. Trenkle, Corinne E. Packard, and Christopher A. Schuh, Rev. Sci. Instrum., 81 (7), 073901 (2010).
[12]	J. M. Wheeler, R. A. Oliver and T. W. Clyne, Diamond Relat. Mater. 19 (11), 1348 (2010).
[13]	Anthony C. Fisher-Cripps, “Nanoindentation”, Springer., 257 (2011).3.
[14]	A. M. Minor, E. T. Lilleodden, E. A. Stachand J. W. Morris., J. Mater. Res., 19, 176 (2004).
[15]	Payel Maiti, Ammar Eqbal, Manjima Bhattacharya, Pradip Sekhar Das, Jiten Ghosh, Anoop Kumar Mukhopadhyay, Ceram. Int., 45 (7), 8204 (2019).

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APA Style

Toshiro Okawa, Ian Thomas Clark, Katsuhiko Tashiro, Hideo Honma, Kazuhiro Yoshihara, et al. (2019). Area Function for Nanoindentation at High Temperatures. International Journal of Materials Science and Applications, 8(6), 98-102. https://doi.org/10.11648/j.ijmsa.20190806.11

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ACS Style

Toshiro Okawa; Ian Thomas Clark; Katsuhiko Tashiro; Hideo Honma; Kazuhiro Yoshihara, et al. Area Function for Nanoindentation at High Temperatures. Int. J. Mater. Sci. Appl. 2019, 8(6), 98-102. doi: 10.11648/j.ijmsa.20190806.11

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AMA Style

Toshiro Okawa, Ian Thomas Clark, Katsuhiko Tashiro, Hideo Honma, Kazuhiro Yoshihara, et al. Area Function for Nanoindentation at High Temperatures. Int J Mater Sci Appl. 2019;8(6):98-102. doi: 10.11648/j.ijmsa.20190806.11

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@article{10.11648/j.ijmsa.20190806.11,
  author = {Toshiro Okawa and Ian Thomas Clark and Katsuhiko Tashiro and Hideo Honma and Kazuhiro Yoshihara and Osamu Takai},
  title = {Area Function for Nanoindentation at High Temperatures},
  journal = {International Journal of Materials Science and Applications},
  volume = {8},
  number = {6},
  pages = {98-102},
  doi = {10.11648/j.ijmsa.20190806.11},
  url = {https://doi.org/10.11648/j.ijmsa.20190806.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20190806.11},
  abstract = {It becomes important to measure mechanical properties of local area of materials because of downsizing of industrial materials, and the fracture of materials often starts at the nanoscale defects. Therefore, the measurement of hardness of the local area of materials is one of key technologies to develop new materials. Nanoindentation is the depth sensing indentation method and can measure the mechanical properties of nanoscale area of materials. The hardness of materials under the controlled environment like high temperature is a big issue in energy or environment industries. Therefore, it becomes important to measure high temperature mechanical properties of nanoscale area of materials by nanoindentation. However, the shape of indenter may change when an indenter contacts to the material surface at high temperatures, and the nanoindentation at high temperatures may lead to inaccuracy of measurements. Nanoindentation does not measure indented are directly but converts the indentation depth to the indented area by area function. In order to correctly convert the indentation depth to the indented area, it is necessary to derive the area function of indented area at high temperatures. In this report, the area function is proposed that considers the change of indenter shape during repeating contact at heated materials. By using this proposed area function, nanoindentation hardness and the reduced modulus of sapphire were obtained at 303K, 473K, 673K, 873K and 1073K successfully. The nanoindentation can be used at high temperatures, if this proposed area function is used.},
 year = {2019}
}

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TY  - JOUR
T1  - Area Function for Nanoindentation at High Temperatures
AU  - Toshiro Okawa
AU  - Ian Thomas Clark
AU  - Katsuhiko Tashiro
AU  - Hideo Honma
AU  - Kazuhiro Yoshihara
AU  - Osamu Takai
Y1  - 2019/10/31
PY  - 2019
N1  - https://doi.org/10.11648/j.ijmsa.20190806.11
DO  - 10.11648/j.ijmsa.20190806.11
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 98
EP  - 102
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20190806.11
AB  - It becomes important to measure mechanical properties of local area of materials because of downsizing of industrial materials, and the fracture of materials often starts at the nanoscale defects. Therefore, the measurement of hardness of the local area of materials is one of key technologies to develop new materials. Nanoindentation is the depth sensing indentation method and can measure the mechanical properties of nanoscale area of materials. The hardness of materials under the controlled environment like high temperature is a big issue in energy or environment industries. Therefore, it becomes important to measure high temperature mechanical properties of nanoscale area of materials by nanoindentation. However, the shape of indenter may change when an indenter contacts to the material surface at high temperatures, and the nanoindentation at high temperatures may lead to inaccuracy of measurements. Nanoindentation does not measure indented are directly but converts the indentation depth to the indented area by area function. In order to correctly convert the indentation depth to the indented area, it is necessary to derive the area function of indented area at high temperatures. In this report, the area function is proposed that considers the change of indenter shape during repeating contact at heated materials. By using this proposed area function, nanoindentation hardness and the reduced modulus of sapphire were obtained at 303K, 473K, 673K, 873K and 1073K successfully. The nanoindentation can be used at high temperatures, if this proposed area function is used.
VL  - 8
IS  - 6
ER  -

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Author Information

Toshiro Okawa

Scienta Omicron, Inc., Tokyo, Japan
Ian Thomas Clark

Seiko Epson Corporation, Nagano, Japan
Katsuhiko Tashiro

Materials & Surface Engineering Research Institute, Kanto Gakuin University, Kanagawa, Japan
Hideo Honma

Materials & Surface Engineering Research Institute, Kanto Gakuin University, Kanagawa, Japan
Kazuhiro Yoshihara

National Institute for Material Science, Ibaraki, Japan
Osamu Takai

Materials & Surface Engineering Research Institute, Kanto Gakuin University, Kanagawa, Japan

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Plain Text BibTeX RIS

APA Style

Toshiro Okawa, Ian Thomas Clark, Katsuhiko Tashiro, Hideo Honma, Kazuhiro Yoshihara, et al. (2019). Area Function for Nanoindentation at High Temperatures. International Journal of Materials Science and Applications, 8(6), 98-102. https://doi.org/10.11648/j.ijmsa.20190806.11

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ACS Style

Toshiro Okawa; Ian Thomas Clark; Katsuhiko Tashiro; Hideo Honma; Kazuhiro Yoshihara, et al. Area Function for Nanoindentation at High Temperatures. Int. J. Mater. Sci. Appl. 2019, 8(6), 98-102. doi: 10.11648/j.ijmsa.20190806.11

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AMA Style

Toshiro Okawa, Ian Thomas Clark, Katsuhiko Tashiro, Hideo Honma, Kazuhiro Yoshihara, et al. Area Function for Nanoindentation at High Temperatures. Int J Mater Sci Appl. 2019;8(6):98-102. doi: 10.11648/j.ijmsa.20190806.11

Copy | Download

@article{10.11648/j.ijmsa.20190806.11,
  author = {Toshiro Okawa and Ian Thomas Clark and Katsuhiko Tashiro and Hideo Honma and Kazuhiro Yoshihara and Osamu Takai},
  title = {Area Function for Nanoindentation at High Temperatures},
  journal = {International Journal of Materials Science and Applications},
  volume = {8},
  number = {6},
  pages = {98-102},
  doi = {10.11648/j.ijmsa.20190806.11},
  url = {https://doi.org/10.11648/j.ijmsa.20190806.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20190806.11},
  abstract = {It becomes important to measure mechanical properties of local area of materials because of downsizing of industrial materials, and the fracture of materials often starts at the nanoscale defects. Therefore, the measurement of hardness of the local area of materials is one of key technologies to develop new materials. Nanoindentation is the depth sensing indentation method and can measure the mechanical properties of nanoscale area of materials. The hardness of materials under the controlled environment like high temperature is a big issue in energy or environment industries. Therefore, it becomes important to measure high temperature mechanical properties of nanoscale area of materials by nanoindentation. However, the shape of indenter may change when an indenter contacts to the material surface at high temperatures, and the nanoindentation at high temperatures may lead to inaccuracy of measurements. Nanoindentation does not measure indented are directly but converts the indentation depth to the indented area by area function. In order to correctly convert the indentation depth to the indented area, it is necessary to derive the area function of indented area at high temperatures. In this report, the area function is proposed that considers the change of indenter shape during repeating contact at heated materials. By using this proposed area function, nanoindentation hardness and the reduced modulus of sapphire were obtained at 303K, 473K, 673K, 873K and 1073K successfully. The nanoindentation can be used at high temperatures, if this proposed area function is used.},
 year = {2019}
}

Copy | Download

TY  - JOUR
T1  - Area Function for Nanoindentation at High Temperatures
AU  - Toshiro Okawa
AU  - Ian Thomas Clark
AU  - Katsuhiko Tashiro
AU  - Hideo Honma
AU  - Kazuhiro Yoshihara
AU  - Osamu Takai
Y1  - 2019/10/31
PY  - 2019
N1  - https://doi.org/10.11648/j.ijmsa.20190806.11
DO  - 10.11648/j.ijmsa.20190806.11
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 98
EP  - 102
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20190806.11
AB  - It becomes important to measure mechanical properties of local area of materials because of downsizing of industrial materials, and the fracture of materials often starts at the nanoscale defects. Therefore, the measurement of hardness of the local area of materials is one of key technologies to develop new materials. Nanoindentation is the depth sensing indentation method and can measure the mechanical properties of nanoscale area of materials. The hardness of materials under the controlled environment like high temperature is a big issue in energy or environment industries. Therefore, it becomes important to measure high temperature mechanical properties of nanoscale area of materials by nanoindentation. However, the shape of indenter may change when an indenter contacts to the material surface at high temperatures, and the nanoindentation at high temperatures may lead to inaccuracy of measurements. Nanoindentation does not measure indented are directly but converts the indentation depth to the indented area by area function. In order to correctly convert the indentation depth to the indented area, it is necessary to derive the area function of indented area at high temperatures. In this report, the area function is proposed that considers the change of indenter shape during repeating contact at heated materials. By using this proposed area function, nanoindentation hardness and the reduced modulus of sapphire were obtained at 303K, 473K, 673K, 873K and 1073K successfully. The nanoindentation can be used at high temperatures, if this proposed area function is used.
VL  - 8
IS  - 6
ER  -

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